然后研究了三氟甲磺酸镱催化的胺和乙酸乙酯的反应,从而合成了乙酰苯胺类化合物。
Objective:To study the anti tumor effects of Sorbaria sorbifolia ethyl acetate extract and its mechanism.
方法以1,3-溴丙烷与乙酰乙酸乙酯为原料经环合、开环、溴代等反应合成。
METHODS The compound was synthesized through the reaction of cyclization, split, bromination et al and using 1,3-propyl bromide and ethyl acetoacetate as raw materials.
该结果对乙酰乙酸酯法合成假性紫罗兰酮的工业开发具有实用价值。
The results can be used to guide the engineering development for the synthesis of pseudoionone by this method.
以乙酰乙酸叔丁酯为原料,经过肟化、醚化、氯代酯解反应合成了头孢克肟开环侧链酸。
Cefixime open side chain acid was prepared by oximation, etherification, chlorination, ester decomposition using t-butyl acetoacetate as starting material.
西司他丁钠的合成以乙酰乙酸乙酯和1-溴-5-氯戊烷为原料,经活性亚甲基烃化、成肟和水解3步反应得7-氯-2-氧庚酸乙酯;
The synthesis of Cilastatin sodium started from ethyl acetoacetate and 1-bromo-5-chloropentane, through 3 steps to produce ethyl 7-chloro-2-oxoheptanoate;
西司他丁钠的合成以乙酰乙酸乙酯和1-溴-5-氯戊烷为原料,经活性亚甲基烃化、成肟和水解3步反应得7-氯-2-氧庚酸乙酯;
The synthesis of Cilastatin sodium started from ethyl acetoacetate and 1-bromo-5-chloropentane, through 3 steps to produce ethyl 7-chloro-2-oxoheptanoate;
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