并按质量标准研究的技术要求,对药材及制剂进行了系统的鉴别、检查、浸出物测定及含量测定等项研究。
According to the technical demands of quality standard of new drug, the author has studied systematic identification test of extraction and content assay of Rhiroma Menipermi.
测定其水溶性浸出物和吸湿性,及其堆密度、休止角,考察其填充性和流动性状况。
Measure water soluble extract and humidity-absorption, pile concentration and dormant Angle, investigate its fill and flow.
采用药典方法分别测定浸出物、总灰分和酸不溶性灰分和进行重金属检查,综合考察不同产地地龙的内在质量。
Pharmacopeia method was used in water soluble extractives and limit test for heavy metals and total ash and acid-insoluble ash to test the quality in Lumbricus from different origin.
方法采用化学鉴别、光谱分析及比色法等方法,对白鹤灵芝的化学成分进行分析及浸出物含量测定。
Mehtods The methods of chemical identification, spectral analysis and colorimetry were used to assay the chemical components and extracts of Rhinacanthus Nasutus.
方法:采用砂烫法进行水浸出物含量测定。
Methods: We measured the content of water-soluble lixivium by means of sand-scorch.
方法:按《中国药典》2005年版一部附录的方法测定水分、总灰分、酸不溶灰分和浸出物。
Methods: the water content, total ashes, insoluble in acids ashes and extracts were determined according to the approaches listed in the Chinese Pharmacopeoa published in 2005.
方法:通过正交实验,以黄芪甲苷、总浸出物为指标,采用HPLC等方法测定指标成分的含量,综合评价酶解工艺的优劣。
Methods: Regarding astragaloside and total extract as indexes, use orthogonal experiments to determine the content of the index ingredient by HPLC.
方法:用薄层色谱鉴别颗粒剂中的麦冬、金银花,测定醇性浸出物,并考察本品的稳定性。
Method: TLC was used to test Radix Ophzopogonis and Flos Lonicerae, and assaying the alcohol extraction, as well as the granule stability.
方法:采用中国药典(2005版)的方法进行醇溶性浸出物、总灰分、酸不溶灰分的测定;
Methods:The alcohol-soluble extracts, ash and acid insoluble ash were determined respectively by the methods issued in the Pharmacopoeia(2005 edition)of the People's Republic of China.
结论建立了黄褐毛忍冬鉴别、浸出物、含量测定方法,能有效用于黄褐毛忍冬质量控制,为黄褐毛忍冬质量标准提高提供实验依据。
These methods can effectively control the quality of Lonicera fulvotomentosa and so that they can supply the experiment basis for improving the quality standard of Lonicera fulvotomentosa.
结论建立了黄褐毛忍冬鉴别、浸出物、含量测定方法,能有效用于黄褐毛忍冬质量控制,为黄褐毛忍冬质量标准提高提供实验依据。
These methods can effectively control the quality of Lonicera fulvotomentosa and so that they can supply the experiment basis for improving the quality standard of Lonicera fulvotomentosa.
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