Carboxylic crosslinked polystyrene microsphere was prepared by F-C acylation reaction.
通过傅克酰基化反应制备了羧基化交联聚苯乙烯微球。
The diacetyl fluorescein was synthesized through the acylation reaction with industry fluorescein.
用工业级荧光素，经过酰化反应合成双乙酰荧光素。
X-ray photoelectron spectroscopy was employed to analyze the surface chemical properties of specimens of acid treatment and acylation reaction.
利用X射线光电子能谱对酸氧化及酰氯化处理后的样品进行了表面化学性质分析。
Methods One compound was synthesized by using caffeic acid as raw materials through the reaction of acylation, esterification, hydrolysis, and so on.
方法以咖啡酸为起始原料，经过酰化、酯化、水解等反应进行合成。
METHODS: The title compounds were synthesized by acylation of twelve acyl chlorides and two intermediates prepared by Friedel Crafts reaction, lengthening of carbon chain, hydrolysis and cyclization;
方法：通过付克反应、碳链延长、水解和环合反应得到两个关键中间体，然后通过酰化反应制得各种酰胺化合物；
Currently, the reaction progress monitoring focuses on amide acylation and deprotection reaction, while there is no method for the reaction progress of the intermediate-active esters.
目前，合成过程的中间监测方法主要集中在胺酰化及脱保护反应，而对于中间体一活化酯的反应进程没有监测方法。
Methods and results:Through acylation, Friedel Crafts reaction, reduction, hydrolysis, condensation and oxidation, the title compound was prepared with a total yield of 50.7%.
方法：以庚二酸单乙酯为原料，经酰氯化、傅克酰化、还原、水解、缩合及氧化反应合成塞曲司特。结果：塞曲司特的总产率为5 0 .7%。
Methods and results:Through acylation, Friedel Crafts reaction, reduction, hydrolysis, condensation and oxidation, the title compound was prepared with a total yield of 50.7%.
方法：以庚二酸单乙酯为原料，经酰氯化、傅克酰化、还原、水解、缩合及氧化反应合成塞曲司特。结果：塞曲司特的总产率为5 0 .7%。
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