Based on it, the synthesis method has been improved. Several new compounds have been prepared by the Grignard reaction of its hydrogenation product.
在此基础上，改进了它的合成方法，并通过它的氢化产物的格氏反应，制备了一些新的化合物。
According to the mechanism of the exchange of metal-halogen, the time and temperature of reaction is proper extended, and the quality of reaction of grignard is improved.
根据金属—卤素交换的机理，适当的延长时间和降低温度，使格利雅合成的质量得到提高。
The synthesis methods of hexamethyldisilane, such as reductive coupling reaction, Grignard reagent alkylation, electrochemical reduction et al, were recounted in details.
综述了近年来国外关于六甲基二硅烷的合成工艺（还原耦合法、格氏试剂法、电解还原法等）；并就其未来的研究方向提出了建议。
Diallylethoxylmethylsilane is an important silicone intermediate. It was prepared by reaction of methyltriethoxylsilane with allyl chloride grignard reagent.
甲基二烯丙基硅烷是一种重要的有机硅中间体，采用甲基三乙氧基硅烷和烯丙基氯通过格式反应制得。
Diallylethoxylmethylsilane is an important silicone intermediate. It was prepared by reaction of methyltriethoxylsilane with allyl chloride grignard reagent.
甲基二烯丙基硅烷是一种重要的有机硅中间体，采用甲基三乙氧基硅烷和烯丙基氯通过格式反应制得。
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