Aim \ Enanthal diethyl acetal is prepared with heptaldehyde and triethyl orthoformate as raw materials.
目的研究以庚醛和原甲酸三乙酯为原料制备庚醛二乙缩醛的工艺条件。
Cyclohexanone diethyl acetal was prepared from cyclohexanone with anhydrous ethanol as reactant, ammonium chloride as catalyst, triethyl orthoformate as water scavenger.
其制备方法是以氯化铵为催化剂，原甲酸三乙酯为解水剂，由无水乙醇和环己酮缩合合成。
METHODS 5-amino-1-hydroxyethyl pyrazole-4-carboylic acid was synthesized through condensation of ethyl cyanoacetate and triethyl orthoformate followed by one-pot methodology of cyclization, hydolysis.
方法原甲酸三乙酯与氰乙酸乙酯缩合，然后和羟乙基肼经环合、水解等一锅法合成5-氨基吡唑-4-甲酸，然后在亚硫酸钠存在条件下加热脱羧得到5-氨基-1-羟乙基吡唑。
METHODS 5-amino-1-hydroxyethyl pyrazole-4-carboylic acid was synthesized through condensation of ethyl cyanoacetate and triethyl orthoformate followed by one-pot methodology of cyclization, hydolysis.
方法原甲酸三乙酯与氰乙酸乙酯缩合，然后和羟乙基肼经环合、水解等一锅法合成5-氨基吡唑-4-甲酸，然后在亚硫酸钠存在条件下加热脱羧得到5-氨基-1-羟乙基吡唑。
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