• Methods and results:Through acylation, Friedel Crafts reaction, reduction, hydrolysis, condensation and oxidation, the title compound was prepared with a total yield of 50.7%.

    方法:以庚二酸单乙酯原料,氯化、傅克酰化、还原、水解、缩合氧化反应合成塞曲司特。结果:塞曲司特总产率为5 0 .7%。

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  • METHODS: The title compounds were synthesized by acylation of twelve acyl chlorides and two intermediates prepared by Friedel Crafts reaction, lengthening of carbon chain, hydrolysis and cyclization;

    方法通过付克反应延长水解环合反应得到两个关键中间体,然后通过化反应制得各种酰胺化合物

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  • The key steps, Friedel-Crafts reaction and Fremy's salt oxidation, were improved on the basis of original literature.

    关键步骤弗-克反应弗瑞麦氏氧化反应文献基础上作了相应的改进

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  • The tertiary butyl benzene synthesis is a supplement to alkylation of classical Friedel and Crafts reaction.

    合成的新工艺的实施,经典“弗德-克来福特”反应中烷基化的补充

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  • The distribution of the isomers of the product and the disproportionated product of alkyl-benzene in the FriedelCrafts reaction have been determined.

    并对反应产物异构体分布及异丁苯的歧化反应做了分析。

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  • Propiophenone is a important intermediate in organic synthesis. It has been prepared in some methods. One of them is Friedel-Crafts reaction.

    丙酮重要有机合成中间体已有多种方法合成,其中之一是付瑞德尔—克拉夫慈反应。

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  • But traditional Friedel-Crafts reaction has its own limitations, such as requirement of a stoichiometric amount of Lewis acid catalysts and large amounts of undesired products.

    传统傅克反应局限性在于,需要等量路易斯催化剂产生大量的副产物

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  • Results showed that the experimental conditions of the Friedel-Crafts Reaction and the water contents of the resin have a significant influence on its adsorption capacity.

    结果显示,二次交反应条件树脂含水量吸附能力具有较大影响

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  • The post-crosslinking fiber was prepared by cross-linking PP-ST-DVB fiber with p-xylylenedichloride according to the friedel-crafts reaction and was given a series of synthesis tests.

    二氯甲基苯作为后联剂,聚丙烯接枝苯乙烯-乙烯苯纤维进行后交联反应制备出具有高比表面积后交联纤维。

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  • The post-crosslinking fiber was prepared by cross-linking PP-ST-DVB fiber with p-xylylenedichloride according to the friedel-crafts reaction and was given a series of synthesis tests.

    二氯甲基苯作为后联剂,聚丙烯接枝苯乙烯-乙烯苯纤维进行后交联反应制备出具有高比表面积后交联纤维。

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