ConclusionThe co-utilization of silica gel column and gel chromatography can greatly improve the efficiency of isolation and purification.
结论硅胶柱色谱和凝胶柱色谱的混合利用可以提高供试品的分离纯化效果。
METHODS ? The isolation and purification was performed by silica gel column chromatography and the structures were identified by spectral analysis.
用硅胶柱层析法分离纯化，用光谱法进行结构鉴定。
Methods:The isolation and purification were carried out by repeated silica gel column chromatography, and the chemical structures were determined by physicochemical properties and spectral analysis.
方法：采用反复硅胶柱色谱、葡聚糖凝胶色谱等分离纯化，通过理化常数和波谱分析鉴定其化学结构。
Method: Isolation and purification of the trace constituents were carried out mainly by solvents extraction and macroporous adsorbing resin and silica gel column chromatography.
方法：用纯净水提取，溶剂萃取，大孔吸附树脂和硅胶柱色谱分离等方法分离并纯化亚麻根的微量成分，通过波谱分析鉴定化合物的结构。
Method: Isolation and purification of the trace constituents were carried out mainly by solvents extraction and macroporous adsorbing resin and silica gel column chromatography.
方法：用纯净水提取，溶剂萃取，大孔吸附树脂和硅胶柱色谱分离等方法分离并纯化亚麻根的微量成分，通过波谱分析鉴定化合物的结构。
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