The effects of solvent of Grignard reagent, pyridine hydrochloride and boron tribromide on yield of product were investigated.
考察了格氏试剂的溶剂、反应物盐酸吡啶和三溴化硼对脱甲氧基收率的影响。
The synthesis methods of hexamethyldisilane, such as reductive coupling reaction, Grignard reagent alkylation, electrochemical reduction et al, were recounted in details.
综述了近年来国外关于六甲基二硅烷的合成工艺（还原耦合法、格氏试剂法、电解还原法等）；并就其未来的研究方向提出了建议。
Study the technologic conditions of preparing Grignard reagent benzylmagnesium chloride under ultrasonic condition.
研究超声波法制备格利雅试剂氯化苄基镁的工艺条件。
Through experiment we discussed the preparative condition and came out with methods of mono-Grignard Reagent preparation.
通过实验讨论了它们的制备条件，提出了单格氏试剂的两种制备方法。
The decyl chloride was used instead of 1-bromodecane to produce Grignard reagent to reduce production of the byproduct eicosane;
以氯癸烷替代溴癸烷做格氏反应，有效地降低了偶联副产物的生成；
The decyl chloride was used instead of 1-bromodecane to produce Grignard reagent to reduce production of the byproduct eicosane;
以氯癸烷替代溴癸烷做格氏反应，有效地降低了偶联副产物的生成；
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