• 比较了氯乙酰乙酰溴中间体硝基安定收率影响

    The effect of chloroacetyl chloride and bromoacetyl bromide on yields of intermediates and nitrazepam was compared.

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  • 托纳博沙种抑制CSD的二乙基乙酰胺间隙结合阻滞剂曾被认为是一种能防止偏头痛的的化合物

    Tonabersat is a neuronal gap-junction blocker that inhibitsCSD and was once considered a promising new compound to preventmigraine attacks.

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  • 采用正丁醇-氢氧化钠反应体系,以十六烷基三甲基化铵转移催化剂乙酰为92%壳聚糖

    The chitosan was prepared with 92% deacetylation degree using n-butanol and sodium hydroxide as a reaction medium and cetyltrimethylammonium bromide as a phase transfer catalyst.

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  • 光照加速乙酰降解

    Light could accelerate the degradation of BA.

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  • 结构红外光谱核磁共振谱元素分析证明2乙酰基—7—甲胺基—4—革酮。

    The structure of the product was proved by IR, HNMR and elemental analysis. That is 2 -acetyl - 7 -methylamino -4-bromotropone.

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  • 柱前衍生试剂,建立了高效液相色谱法间接测定2-乙酰氧基异丁酰新方法。

    A rapid reverse high performance liquid chromatography method based on the iso - propyl alcohol as an agent of pre-derivatization is developed for the determination of 2-acetoxyisobutyryl bromide.

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  • 用薄层色谱监测乙酰丙酸乙酯生成3-乙酰丙酸乙酯反应过程优化了反应条件,方法简单,快速,准确。

    A simple TLC method for monitoring the synthetic process of 3-bromo-ethyl levulinate is reported, and the reaction condition is optimized.

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  • 结果表明土壤碱性愈有机物质含量乙酰土壤中的降解愈快

    The results showed that:the more stronger the alkalinity of the soil was, the more higher the levels of organic compounds in the soil was, the more rapidly the BA was degraded in the soil.

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  • 植物水解碱酯酶的区别在于它们不能催化乙酰胆碱化硫代乙酰胆碱水解。

    But they differ from cholinesterase in that they do not catalytically hydrolyze acetylcholine bromide or butylcholine bromide at pH 7—8.

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  • 方法1,3-丙烷乙酰乙酸乙酯原料环合、开环、反应合成

    METHODS The compound was synthesized through the reaction of cyclization, split, bromination et al and using 1,3-propyl bromide and ethyl acetoacetate as raw materials.

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  • 乙酰土壤残留化合物

    BA was a shortterm residual compound in the soil.

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  • 西他丁合成乙酰乙酸1--5-氯戊烷为原料,活性亚甲基烃化、成肟和水解3反应得7-氯-2-氧庚酸乙酯;

    The synthesis of Cilastatin sodium started from ethyl acetoacetate and 1-bromo-5-chloropentane, through 3 steps to produce ethyl 7-chloro-2-oxoheptanoate;

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  • 1,3-二甲基金刚烷为原料,化、硫酸的作用下乙酰胺基化、水解、成盐等反应及改进的后处理方法得到盐酸美金刚,收率6 7。8%。

    Memantine hydrochloride was synthesized from 1,3 dimethyladamantane by bromination, acetamidation with acetonitrile in sulfuric acid and hydrolysis with an overall yield of 67.8%.

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  • 1,3-二甲基金刚烷为原料,化、硫酸的作用下乙酰胺基化、水解、成盐等反应及改进的后处理方法得到盐酸美金刚,收率6 7。8%。

    Memantine hydrochloride was synthesized from 1,3 dimethyladamantane by bromination, acetamidation with acetonitrile in sulfuric acid and hydrolysis with an overall yield of 67.8%.

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