The effects of composition of mobile phase, the structure of solute and the column temperature on chiral separation were extensively studied. The chiral recognition mechanism was discussed.
考察了流动相组成、溶质结构和柱温对对映体分离的影响,并初步探讨了手性识别的机理。
A test is carried out after homogenate is filled into the chromatogram column, thus successfully separating chiral medicine ibuprofen enantiomers with a separation degree of 2.03.
匀浆填充成色谱柱后对其进行了测试,成功分离了手性药物布洛芬对映体,其分离度为2.03。
A cinchonine imprinted chiral monolithic column was prepared for the separation of the diastereomers of cinchonine and cinchonidine by in situ molecular imprinting technique.
采用原位分子印迹技术,单步制备了一种辛可宁印迹的手性整体柱。
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