The regioselective nitration of toluene and chlorobenzene with nitrates and supported nitrates on solid acid catalysts and supports in the presence of acetic anhydride is studied.
该文讨论了应用固体酸催化剂和载体,在醋酐存在下,采用硝酸盐和载体硝酸盐硝化甲苯和氯苯的选择性。
METHODS: Potentiometric titration was adopted to determine the content of terbinafine hydrochloride using glacial acetic acid as solvent, acetic anhydride instead of mercury acetate.
方法:采用电位滴定法,以冰醋酸为溶剂,用适量醋酐代替现行标准中使用的醋酸汞,建立了测定盐酸特比萘芬原料药含量的方法;
Sulfuric acid and acetic anhydride were used as a cyclizing agent to prepare Ofloxacin intermediate. The reaction could be carried out under moderate conditions and facilitate industrial produce.
用硫酸乙酐混合物作环合剂,制备了氟嗪酸中间体.该方法具有反应条件温和、价格便宜、后处理简单的优点,适用于工业化生产。
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