The preparation method and conditions of the catalysts are cocurrent precipitation and immediate filtration;
3
反应后蒸馏出多余甲醇,反应液相趁热过滤,分离出催化剂,然后将滤液静置过夜分层。
Distilling excessive menthol after reaction, filtering the liquid phase at a high temperature, separating the catalyst, stewing the filtrate for overnight stratification.