... 甲醇溶解试验Solubility in Methanol 结晶点crystallization point 乙醇溶解试验solubility in ethanol ...
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Melting point and crystallization point of the raw products were measured, melting point 49.8℃, crystallization point 47.48℃. The stability and repetition of the synthesis experiment were measured and were satisfying, average yield of products in these experiments was over 95%.
在该工艺条件下，氯苯转化率可达100％，反应选择性为95.4％，以氯苯量计，产率为95.4％，粗产品中2，4-二硝基氯苯含量为96.39％；对粗产品的熔点和结晶点进行了测定，其熔点为49.8℃，结晶点为47.48℃；对合成实验的重复性和稳定性进行了验证，其产率均在95％以上，实验的稳定性和重复性较好。
参考来源 - 连续绝热硝化合成2，4·2,447,543篇论文数据，部分数据来源于NoteExpress
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