甲基丙烯酸缩水甘油酯的合成研究 关键词: 甲基丙烯酸缩水甘油酯; 相转移催化剂; 合成; 纯化[gap=623]Key words: glycidyl methacrylate; the phase transfer catalyst; synthesis; purification
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The yield was increased through adding tetrabutyl ammonium bromide as the phase transfer catalyst, and using excessive diisopropyl phosphite to compensate its hydrolyzation.
通过添加适量四丁基溴化铵为相转移催化剂,使用过量的亚磷酸二异丙酯以补偿其在强碱环境中的水解,从而提高了反应产率。
The phase transfer catalyst Ql can be repeatedly used.
相转移催化剂可反复使用。
CONCLUSION The phase transfer catalyst has advantages of simple starting material, convenient operations and mild reaction conditions.
相转移法合成萘丁美酮具有所用试剂易得,操作方法简便,反应条件温和,成本较低等优点。
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