The yield was increased through adding tetrabutyl ammonium bromide as the phase transfer catalyst, and using excessive diisopropyl phosphite to compensate its hydrolyzation.
通过添加适量四丁基溴化铵为相转移催化剂,使用过量的亚磷酸二异丙酯以补偿其在强碱环境中的水解,从而提高了反应产率。
The phase transfer catalyst Ql can be repeatedly used.
相转移催化剂可反复使用。
CONCLUSION The phase transfer catalyst has advantages of simple starting material, convenient operations and mild reaction conditions.
相转移法合成萘丁美酮具有所用试剂易得,操作方法简便,反应条件温和,成本较低等优点。
CONCLUSION The phase transfer catalyst has advantages of simple starting material, convenient operations and mild reaction conditions.
相转移法合成萘丁美酮具有所用试剂易得,操作方法简便,反应条件温和,成本较低等优点。
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